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    STUDIA PHYSICA - Issue no. 1 / 2016  
         
  Article:   Fe2O3 PARTICLES AS PRECURSORS FOR α”-Fe16N2 PHASE SYNTHESIS.

Authors:  V. POP.
 
       
         
  Abstract:  

Published Online: 2016-06-01
Published Print: 2016-06-30

VIEW PDF: Fe2O3 PARTICLES AS PRECURSORS FOR α”-Fe16N2 PHASE SYNTHESIS

In this work we investigate the structural properties and microstructure of Fe2O3 particles synthesized using the sol-gel method. Differential thermal and thermogravimetric analysis showed that the organic matrix is completely burned off at temperatures higher than 520 °C. The sample annealed at 550 °C for 12 h contained only the Fe2O3 phase. The obtained hematite particles are micrometer sized and have an elongated shape. Taking into account the cheap and available sol-gel precursors, the possibility of using these particles in α”-Fe16N2 synthesis is discussed.

Keywords: Hematite, Sol-gel synthesis, Shape anisotropy, X-ray Diffraction, Calorimetry, Annealing.
 
         
     
         
         
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